Abstract
We have achieved the highly sensitive electrochemical detection of reversible redox species by a new type of stripping analysis name substitutional stripping voltammetry (SSV). This analysis requires an interfigitated army (IDA) microelectrode in a sample solution combined with a microelectrode in a second cell. The second cell contains an electroactive species which deposits reversibly on the electrode. The charge generated by the redox cycling reaction of the sample at the IDA is transmitted to the microelectrode and accumulated by the deposition of metal ion species on the macroelectrode
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