Abstract
A robust, easy to optimize, and efficient homonuclear correlation NMR experiment for half-integer quadrupolar nuclei in solids is described and has been experimentally tested on anhydrous Na2HPO4-(23Na, S= 3/2 nucleus) and as-synthesized AlPO4-14 (27Al, S= 5/2 nucleus), an aluminophosphate molecular sieve.
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