Abstract
Tin(II) dithiolates, Sn[SR] 2 (R = Me, C 6H 13, C 7H 15 CH 2Ph, Ph, p-tolyl), and the tin((II)-sulphur heterocycles Sn.S.CH 2.CH 2S and Sn.S.C 6H 4Me.S , have been synthesised by the protolysis of the tin(II)-carbon bond by thiols. Tin-119m Mössbauer and infra-red spectra are reported, and the structures of the compounds discussed. 2-Thioethanol reacts similarly to give tin(II)di(2-thioethoxide) and not the expected heterocycle Sn.S.CH 2CH 2O .
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