Abstract
Abstract 1-Substituted F-1-alkenyl phosphates, prepared easily from F-alkyl ketones, were treated with diisobutylaluminium hydride in tetrahydrofuran at 0 °C for 5 min or at room temperature for 30 min to generate quantitatively the corresponding ketone aluminium(III) enolates, which underwent the aldol reaction with various aldehydes at 0 °C to give α-fluoro-α-F-alkyl β-hydroxy ketones in good to excellent yields.
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