Abstract

The purpose of this study was to evaluate whether the incorporation of an acidic monomer into the pulp-capping material TheraCal LC, which has a weak dentin bonding, increases the shear bond strength (SBS) to dentin. Di-2-hydroxyethyl methacryl hydrogenphosphate was incorporated into the material at 0.0 (TL0, control), 5.0 (TL5), and 10.0 (TL10) wt%. The water contact angle (CA) and mechanical properties for each material were also studied (n = 6). Debonding was performed at two different times (immediate and after 24 h) (n = 12). Hydroxyl and calcium ion releases in water at 37 °C were monitored up to 28 days (n = 6). The addition of the acidic monomer decreased the CAs (p < 0.001) and increased the flexural moduli (p < 0.001). The debonding time did not significantly affect the SBS values (p = 0.600). The TL10 group exhibited the highest SBS values, followed by the TL5 group. The TL10 group released significantly more calcium ions than the other two groups from 3 days (p < 0.05). The incorporation of the acidic monomer at 10.0 wt% into TheraCal LC enhanced bonding to dentin, while not negatively affecting the mechanical properties and ion-leaching capacity of the material.

Highlights

  • Direct pulp capping involves covering the exposed pulp with a material to preserve its vitality and its functional and biological activities [1]

  • Calcium hydroxide has been used in direct/indirect pulp-capping mainly due to its ability to release hydroxyl and calcium ions on dissolution [1,2]

  • It has been reported that mineral trioxide aggregate (MTA) is more effective than calcium hydroxide due to its enhanced interaction with pulp tissue and fewer negative responses to pulp [1]

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Summary

Introduction

Direct pulp capping involves covering the exposed pulp with a material to preserve its vitality and its functional and biological activities [1]. Calcium hydroxide has been used in direct/indirect pulp-capping mainly due to its ability to release hydroxyl and calcium ions on dissolution [1,2]. Its high solubility, lack of adhesion, and poor physical–chemical properties have recently gained relevance as clinical issues [2]. Mineral trioxide aggregate (MTA) and MTA-derived materials have been suggested as new direct/indirect pulp-capping agents and have shown favorable results in clinical trials [2]. It has been reported that MTA is more effective than calcium hydroxide due to its enhanced interaction with pulp tissue and fewer negative responses to pulp [1].

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