Abstract

Laboratory X-ray diffraction contrast tomography (LabDCT) is a novel imaging technique for non-destructive 3D characterization of grain structures. An accurate grain reconstruction critically relies on precise segmentation of diffraction spots in the LabDCT images. The conventional method utilizing various filters generally satisfies segmentation of sharp spots in the images, thereby serving as a standard routine, but it also very often leads to over or under segmentation of spots, especially those with low signal-to-noise ratios and/or small sizes. The standard routine also requires a fine tuning of the filtering parameters. To overcome these challenges, a deep learning neural network is presented to efficiently and accurately clean the background noise, thereby easing the spot segmentation. The deep learning network is first trained with input images, synthesized using a forward simulation model for LabDCT in combination with a generic approach to extract features of experimental backgrounds. Then, the network is applied to remove the background noise from experimental images measured under different geometrical conditions for different samples. Comparisons of both processed images and grain reconstructions show that the deep learning method outperforms the standard routine, demonstrating significantly better grain mapping.

Highlights

  • Non-destructive 3D characterization of grain structures is indispensable in understanding the microstructural evolution in the bulk of polycrystalline materials

  • By checking slices at other locations, we found that all these grains except grain #693 exist in other sections of both laboratory X-ray diffraction contrast tomography (LabDCT) datasets, indicating a significant spatial shift for reconstructions of these grains

  • We have developed a deep learning (DL) model to clean the background noise of LabDCT images for efficient spot identification

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Summary

Introduction

Non-destructive 3D characterization of grain structures (sizes, shapes and orientations) is indispensable in understanding the microstructural evolution in the bulk of polycrystalline materials. To broaden the use of nondestructive grain mapping by offering such possibilities at home laboratories, laboratory X-ray diffraction contrast tomography (LabDCT) has been developed (King et al, 2013, 2014; McDonald et al, 2015). This novel technique has already been demonstrated to be very useful in 3D/4D studies of metals and alloys (McDonald et al, 2017; Sun et al, 2019, 2020; Lei et al, 2021). It requires extensive human expertise to tune and optimize the processing parameters

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