Abstract
The crystal structure of the title compound, C10H26N2 2+·2NO3 −, exhibits a back-to-back paired double-stacked packing arrangement culminating in an overall double zigzag pattern of the dications. Each pair of double-stacked dications is surrounded by a ring of ten nitrate anions. An intricate three-dimensional N---H...O and N---H...(O,O) hydrogen-bonding network exists in the crystal structure.
Highlights
The crystal structure of the title compound, C10H26N22+2NO3, exhibits a back-to-back paired double-stacked packing arrangement culminating in an overall double zigzag pattern of the dications
An intricate three-dimensional N---H...O and N---H...(O,O) hydrogenbonding network exists in the crystal structure
The structures of many other related n-alkyldiammonium salts are available in the Cambridge Structural Database, see: Allen (2002)
Summary
University of Johannesburg, Department of Chemistry, PO Box 524, Auckland Park, Johannesburg 2006, South Africa. R factor = 0.055; wR factor = 0.157; data-to-parameter ratio = 21.1. The crystal structure of the title compound, C10H26N22+2NO3, exhibits a back-to-back paired double-stacked packing arrangement culminating in an overall double zigzag pattern of the dications. Each pair of double-stacked dications is surrounded by a ring of ten nitrate anions. An intricate three-dimensional N---H...O and N---H...(O,O) hydrogenbonding network exists in the crystal structure. Data collection: SMART-NT (Bruker, 1999); cell refinement: SAINT (Bruker, 2008); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: OLEX2 (Dolomanov et al, 2009 ) and Mercury (Macrae et al, 2006); software used to prepare material for publication: publCIF (Westrip, 2010) and PLATON (Spek, 2009)
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