Abstract
Single crystals of Na 2PdCl 4 show tetragonal symmetry with space group P4/ ncc (No. 130) with four formula units per unit cell. The lattice parameters are a = 9.584(2) A ̊ and c = 7.486(3) A ̊ . The atomic arrangement is explored via X-ray crystal structure analysis. In Na 2PdCl 4 square planar PdCl 4 groups form a complicated three-dimensional atomic arrangement with very distorted NaCl 6-octahedra. The structural relationship between Na 2PdCl 4 and PdBi 2O 4 [1] is discussed.
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