Abstract
Starting from MoCl5 via the intermediates (MeCN)2MoCl4 (1) and (THF)2MoCl4 (2) the tripod complex CH3C(CH2PPh2)3MoCl3 (4) has been synthesized. The yellow cristalline compound 4 has been fully characterized by standard analytical techniques. X-ray-analysis proves the facial coordination of the tripod ligand. To our knowledge 4 is the first Mo(III)-trihalide coordination compound containing three P-donor-ligands in a facial coordination.
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