Abstract
The metallacycle [Br3WS2N3] has been obtained from the reaction of S4N4 with WBr5. The salt [Ph4P+][Br4WS2N3 -] was formed from [Br3WS2N3] by addition of Ph4PBr. It crystallizes in the orthorhombic space group Pbca with a = 1396.8(4), b = 1961.9(5), c = 2108.0(4) pm, and Z = 8. The following mean bond lengths were observed in the anion: W-N 184.2, W-Br 256.8, N-S 157.8 pm.
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