Abstract

The single-distance phase retrieval technique was applied to contrast-enhanced imaging of the dual-phase microstructure of a ferrite/martensite dual-phase with only 1.4% difference in density between the two phases. Each high-resolution absorption-contrast image was registered with a corresponding phase-contrast image, to analyse damage evolution behaviour. The loading step at which each microvoid was nucleated was identified by tracking the microvoid throughout tension, together with its nucleation site. Premature damage initiation was observed at a relatively early stage at various nucleation sites, such as the ferrite interior, martensitic interior and ferrite/martensite interfaces; however, the subsequent growth of such microvoids was relatively moderate. On the other hand, microvoids were also initiated later due to martensitic cracking after the maximum load was reached, and these microvoids subsequently exhibited rapid growth. The martensite cracking induced additional damage evolution mainly along nearby ferrite/martensite interfaces and intersections between the martensite and the ferrite grain boundary. It is notable that the microvoids originating from martensitic cracking exhibited characteristic shear-dominated growth under macroscopic tension, whereas those originating from the other nucleation sites exhibited traditional triaxiality-dominated growth. It was concluded that the ductile fracture was dominated by the substantial force driving the growth of microvoids located on morphologically characteristic martensitic particles.

Highlights

  • The ductile fracture process in alloys consists of nucleation, growth and coalescence of microvoids

  • Combined phase- and absorption-contrast tomography has been applied to a DP steel

  • Growth and coalescence behaviours have been quantitatively investigated by tracking all the microvoids to reveal microstructure/damage evolution relationships under tension

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Summary

INTRODUCTION

The ductile fracture process in alloys consists of nucleation, growth and coalescence of microvoids. The present authors applied the single-distance phase retrieval technique to 3D observations of a DP stainless steel consisting of austenitic and ferritic phases [11,13], and found that a limited number of microvoids, initiated at later stages from fine particles located on ferrite/austenite boundaries, exhibited enormous growth, thereby inducing macroscopic ductile fracture. The modulation transfer function (MTF), derived from the edge response function [18] at the ferrite/martensite interfaces, was measured, in order to determine the spatial resolution at a 5 % contrast ratio in the phase-contrast XMT images It has been reported by the present authors that reasonable agreement was observed between the results of interface-based MTF calculations and those obtained with 3D test patterns [19]. Microvoid nucleation was defined in the present study identically to the previous study [11], where a specific thresholding value in volume expansion (i.e., 1.71 times in volume) is used for detecting microvoid initiation

Damage evolution behaviour
Discussion
Summary
F Microvoid
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