Abstract
In the crystal structure of the title compound [systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide–methanoic acid (1/1)], C16H13NO·CH2O2, the cytenamide and solvent molecules form a hydrogen-bonded R 2 2(8) dimer motif, which is further connected to form a centrosymmetric double-motif arrangement. The asymmetric unit contains two formula units.
Highlights
H atoms treated by a mixture of independent and constrained refinement max = 0.58 e Å 3
H atoms treated by a mixture of independent and constrained refinement w = 1/[σ2(Fo2) + (0.0728P)2 + 0.6562P]
The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry
Summary
The John Arbuthnott Building, University of Strathclyde, 27 Taylor Street, Glasgow G4 0NR, Scotland, bWestCHEM, Department of Pure & Applied Chemistry, University of Strathclyde, 295 Cathedral Street, Glasgow G1 1XL, Scotland, and c. R factor = 0.047; wR factor = 0.142; data-to-parameter ratio = 31.6. In the crystal structure of the title compound [systematic name: 5H-dibenzo[a,d]cycloheptatriene-5-carboxamide–. Methanoic acid (1/1)], C16H13NOCH2O2, the cytenamide and solvent molecules form a hydrogen-bonded R22(8) dimer motif, which is further connected to form a centrosymmetric double-motif arrangement. The asymmetric unit contains two formula units
Sign-in/Register to view highlights & summary Sign-in/Register to access full text options 
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callMore From: Acta crystallographica. Section E, Structure reports online
Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
