Abstract
A 0.1 M solution of sodium trifluoromethanesulfonate in neat trifluoromethanesulfonic (triflic) acid is used as solvent in cyclic voltammetry. Working, counter and quasi-reference electrodes consist of glassy carbon, platinum and silver wire, respectively. Reversible voltammograms between +0.4 and +3 V versus NHE are recorded at 0 °C with scan rates around 100 mV s −1 and are calibrated against Ru- (bpy) 3 3+/2+. Redox processes for a series of coordination compounds involving high oxidation states are studied without complicating chemical reactions.
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