Cyclic Mechanical Fatigue Lifetime of Bi0.5Na0.5TiO3-Based Eco-Piezoceramics.

José F Bartolomé,Álvaro García,Luis E Fuentes-Cobas,Alfredo Jacas,Lorena Pardo

doi:10.3390/ma14154113

Abstract

The mechanical strength and cyclic fatigue behavior of PIC700 commercial eco-piezoceramic disks are investigated under biaxial loading on unpoled and poled samples. The bending strength of unpoled samples was higher than those of poled ones. Fatigue tests were conducted under a load ratio of 10 at a frequency of 20 Hz with a sinusoidal waveform. The curve fitting for the S-N fatigue diagram is used to predict the lifetime of these eco-piezoceramics and describe their fatigue behavior. It was also found that the unpoled samples exhibited higher fatigue resistance than the poled ones. The fatigue limit of maximum load for ten million cycles of unpoled and poled samples was estimated to be 160 and 135 MPa, respectively. The detailed observations of the fatigue fracture surfaces by scanning electron microscopy (SEM) indicated that a wavy surface with a mixture of transgranular and intergranular fractures occurred preferentially in the case of the poled material. On the other hand, transgranular fractures seem to be predominant in the unpoled samples. It appears that the poling process causes the change in failure characteristics due to domain orientation that leaves an anisotropic stress field in the material. The poled ceramics possess a local stress concentration created by the orientation under the electric poling field of the 90° ferroelectric–ferroelastic domains. Under this local stress concentration, a microstructural degeneration is induced by domain switching under the cyclic load that accelerates crack growth, thereby reducing fatigue lifetime.

Highlights

As active elements of piezoelectric devices, piezoceramics are prone to premature failure due to their inherent brittle property under tensile stress and inevitable microstructural inhomogeneities, such as domain walls, grain boundaries, flaws and pores, impurities and inclusions
The results showed that an acceleration of fatigue crack growth occurs as the crack propagates along the domain wall
The cyclic fatigue properties refer to the degradation of mechanical properties of maunpoled sample and the one corresponding to the Rietveld analysis

Summary

Introduction

As active elements of piezoelectric devices, piezoceramics are prone to premature failure due to their inherent brittle property under tensile stress and inevitable microstructural inhomogeneities, such as domain walls, grain boundaries, flaws and pores, impurities and inclusions. It is important to focus on their mechanical properties to ensure long-term serviceability, since the high stability of properties is of key importance in these electronic devices. In some applications, such as energy harvesting from vibrating structures, accelerometers or bending actuators, piezoceramic plates are subjected to cyclic mechanical loads for a long period [1]. The microstructural inhomogeneities cause mechanical discontinuities and induce high stress concentrations, which may induce crack initiation or subcritical crack growth [2]. The study of fatigue crack growth is a key factor to determine the lifetime of these smart ceramic devices

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