Abstract
Tris-(β-cyanoethyl) amine (TCA) and bis-(β-cyanoethyl) amine (DCA) were prepared by silica- mediated aza-Michael reaction of ammonium hydroxide and acrylonitrile in gram scale. First time TCA was used as a stabilizer of Pd(0) nano/microparticles (TCA-Pd) and efficient reagent in water mediated Suzuki cross coupling reaction. Further DCA and TCA were applied as efficient base, ligand (N,N-ligand) and reaction medium in palla- dium-catalyzed Heck cross coupling reaction. © Global Scientific Publishers 2013.
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