Abstract
The first triple-layered borate with edge-sharing BO4 tetrahedra, β-CsB9 O14 was obtained under vacuum-sealed condition. It represents a new structure type and enriches the structural diversity of borates. Moreover, β-CsB9 O14 exhibits a short UV cutoff edge and a large birefringence, indicating that it could be regarded as a DUV birefringent crystal.
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