Abstract
Chemical preparation, X-ray single crystal, thermal analysis and IR spectrometric investigation of (C9H15N3O2)SO4 denoted LTHS are described. The LTHS crystallizes in the monoclinic system with P21 space group. Its unit cell dimensions are a=5.5386(1) Å, b=8.0467(4) Å, c=14.0780(6) Å, β=93.339(3)° with V=626.36(4) Å3 and Z=2. The structure has been solved using direct method and refined to a reliability R factor of 0.0212. The LTHS structure is built up from organic chains parallel to the b axis, linked via NH…O hydrogen bonds and interconnected by inorganic groups so as to build a three-dimensional arrangement.
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