Abstract

1,1′-Azobiscarbamide, C2H4N4O2, is monoclinic, space group P21/c, with a = 3.593, b = 9.095, c = 7.635, β = 113°15′, and Z = 2. Data were collected with an automatic diffractometer using crystal monochromated MoK α radiation. The usual spherical free atom model with anisotropic thermal parameters was used in making the least-squares refinement. In addition, refinements were made with generalized scattering factors, and the scalar, dipole, and quadrupole one-center terms and scalar two-center terms were successively added. The aspherical distortions found are reasonable and produce a significant improvement between measured and calculated intensities. No significant difference in bond distances was observed.

Talk to us

Join us for a 30 min session where you can share your feedback and ask us any queries you have

Schedule a call

Disclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.