Abstract
The title compound crystallizes in space groupP21, with unit cell parametersa = 9.777(1),b = 7.750(1),c= 15.884(2) A, and β = 100.3 °;D c = 1.34 andD m = 1.33 g cm−3 andZ = 2. The structure was solved by direct methods and refined by block-diagonal least-squares procedures with weightedF values to a finalR w of 0.079 (R = 0.084). A total of 2243 intensities was measured, using a diffractometer and monochromated MoKα radiation, of which 826 were ⩽2σ(I) and classed as “unobserved.” In the crystal, the C(10) aryl group is approximately perpendicular to the tetrahydronaphthalene nucleus. The carbon atoms in each of the two sets ofortho-methoxyl groups are in opposition to each other and coplanar with their respective aromatic rings. The methoxyl group attached to the sulfur has an unexplained anomalously short C-O bond length, but otherwise bond lengths and angles are normal.
Talk to us
Join us for a 30 min session where you can share your feedback and ask us any queries you have
Schedule a callDisclaimer: All third-party content on this website/platform is and will remain the property of their respective owners and is provided on "as is" basis without any warranties, express or implied. Use of third-party content does not indicate any affiliation, sponsorship with or endorsement by them. Any references to third-party content is to identify the corresponding services and shall be considered fair use under The CopyrightLaw.
