Crystal structure of diserinesulfate monohydrate

Abstract

The crystal structure of DL-Serine H2SO4 · H2O is determined by single-crystal x-ray diffraction. The intensities of x-ray reflections are measured at three temperatures, namely, 295, 343, and 233 K. The crystal structure of the studied compound is refined using all three sets of intensities. It is demonstrated that, at a temperature of 233 K, the structure transforms into an incommensurately modulated state. This transformation is assumed to be responsible for the disappearance of the piezoresponse at this temperature.