Abstract
The title compound, C17H18O5, was synthesized by a base-free catalytic Wittig reaction. The molecule consists of a diethyl itaconate unit, which is connected via the C=C double bond to a benzofuran moiety. The benzofuran ring system (r.m.s. deviation = 0.007 Å) forms dihedral angles of 79.58 (4) and 12.12 (10)° with the mean planes through the cis and trans ethoxycarbonyl groups, respectively. An intramolecular C—H⋯O hydrogen bond involving the O atom of the benzofuran moiety is observed. In the crystal, molecules are linked into ribbons running parallel to the b axis by C—H⋯O hydrogen bonds.
Highlights
The title compound, C17H18O5, was synthesized by a base-free catalytic Wittig reaction
The molecule consists of a diethyl itaconate unit, which is connected via the C C double bond to a benzofuran moiety
An intramolecular C— HÁ Á ÁO hydrogen bond involving the O atom of the benzofuran moiety is observed
Summary
The title compound, C17H18O5, was synthesized by a base-free catalytic Wittig reaction. V. an der Universitat Rostock, Albert-Einstein-Strasse 29a, 18059 Rostock, Germany. Received 6 October 2015; accepted 12 October 2015 The molecule consists of a diethyl itaconate unit, which is connected via the C C double bond to a benzofuran moiety.
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More From: Acta crystallographica. Section E, Crystallographic communications
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