Abstract
A Np(VII) compound with [Co(en)3]3+ cations, [Co(en)3][NpO4(OH)2]·5H2O (en = ethylenediamine), was synthesized and studied by single crystal X-ray diffraction. The structure consists of [NpO4(OH)2]3– anions and [Co(en)3]3+ cations forming electrically neutral layers, between which water molecules are arranged. A three-dimensional network of hydrogen bonds involving all the constituents of the structure is formed in the crystal. The effect of hydrogen bonding on the geometric characteristics of [NpO4(OH)2]3– anions is discussed.
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