Abstract
A new rubidium zinc oxovanadium phosphate Rb3Zn(VO)2(PO4)(HPO4)(P2O7) has been obtained under hydrothermal conditions. It crystallizes in the P212121 space group with parameters a=7.0989(2) Å, b=9.5374(2) Å, c=23.3016(8) Å. The structure consists of corner-sharing VO6 octahedra, PO4, HPO4, ZnO4 tetrahedra and P2O7 groups leading to layers parallel to (110) interconnected with chains running along a. The open framework that results shows tunnels along a and b where the rubidium atoms are located.
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