Abstract
The compound 4-bromo-3,4-dichloro-1-(1-morpholinyl)-1-(decylsulfanyl)-2-nitro-buta-1,3-diene was synthesized from the reaction of 4-bromo-1,3,4-trichloro-1-(decylsulfanyl)-2-nitro-buta-1,3-diene with morpholine and characterized by elemental analysis, IR spectrum, UV spectra, 1H NMR,13C NMR and X-ray single crystal determination. In the title compound, C18H29BrCl2N2O3S, crystallizes in the monoclinic space group P21/c, a = 15.8326(4) A, b = 8.9915(10) A, c = 16.7528(5) A, β = 100.808(10)°, V = 2,342.6(3) A3, Z = 4, R 1 = 0.0590 and wR 2 = 0.0940. The morpholine ring adopts a chair conformation. The morpholine ring and the butadiene group are inclined at an angle of 113.4 (1)°. The butadiene unit is not planar as can be expected if the two double bonds are fully conjugated. The title compound, C18H29BrCl2N2O3S, crystallizes in the monoclinic space group P21/c. The structure of the compound contains the expected nitro group is substituted to butadienyl skeleton, the alkylsulfanyl chain and the morpholine ring.
Published Version
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