Abstract
Crystals of the title compound are monoclinic with a= 7·459(6), b= 8·694(7), c= 7·915(6)Å, β= 116·6(5)°, space group P21/c and Z= 4. The structure was determined from diffractometer data by symbolic addition procedures, and refined by least-squares methods to R 0·058 for 609 independent reflections. Hydrogen atom positions were also refined. Bond distances are NC 1·122(5), C(sp)–C(sp3) 1·453(5), C(sp3)–C(sp2) 1·524(5), C(sp2)–N 1·330(5), N–N 1·411(5), and CO 1·224(4)Å. The molecules are held together by hydrogen bonds.
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