Abstract
The crystal structure and composition of the ternary (K, Mn, Zr) molybdate were refined using X-ray diffraction data (KM-4 KUMA-Diffraction automatic diffractometer, MoKα radiation, graphite monochromator, ω scan mode, 548 F(hkl), R=0.0427). The unit cell dimensions are a=b=9.474(1), c=24.371(4) A, V=1894.4 A3, Z=6, Ρcalc = 3.337 g/cm3, space group R $$\bar 3$$ c. The crystal structure is a 3D framework of oxygen vertex-sharing (Mn, Zr)O6 octahedra and MoO4 tetrahedra, with potassium atoms located in the large channels; it belongs to the Nasicon structural type.
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