Abstract
In this study, the synthesis, X-ray crystal structure and magnetic properties of a new hexanuclear Fe(III) complex, 2[OFe6(thme)4Cl6].4[C6H15N].6[H2O] (1), (H3thme = 1,1,1-Tris(hydroxymethyl)ethane) is reported. The structure of 1 is described as the hexametalate core [OFe6(thme)4Cl6] consisting of an octahedral arrangement by four alkoxo oxygen atom from thme ligand, a terminal chloride atom and one μ6–oxo group at the center. Variable-temperature magnetic susceptibility measurements of 1 indicate an antiferromagnetic interaction between the Fe(III) centers.
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