Abstract
In the crystal structures of [3 6](1,2,3,4,5,6)cyclophane 1 and the 1:TCNQ (1:1) complex, the cyclophane moiety is observed as the D 6 h structure because of the disorder of the molecules with C 6 h symmetry. In contrast, the C 6 h structure is observed in the crystals of the 1:TCNQ-F 4 (1:1) complex, and the complex shows an alternating donor–acceptor stacking with partial donor–acceptor overlap.
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