Abstract
The chemical preparation and the crystal structure of Ag 6 P 6 O 18 · H 2 O are reported. The title compound is trigonal ( R [unk]) with a = 14.807(10) Å, c = 6.597(7) Å ( a rh = 8.827 Å, α rh = 114.01°), V = 1257(3) Å 3 , Z = 3, M w = 1139.05 amu and D x = 4.515 g cm −3 . The structure has been solved using 1073 independent data with a final R value of 0.035. The P 6 O 18 anions have [unk] symmetry. They alternate along the [unk] axis with rings of six loosely bounded silver atoms. Each Ag 6 ring is connected to its six neighbours by a short Ag – Ag distance (3.003 Å).
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