Abstract
[C15H25N2O2 +·ClO 4 − ,M r =364.83, is monoclinic:P21,a=7.885(1),b=10.685(1),c=10.658(1) A,β=105.63(1)°,V c =864.8(2) A3,Z=2,D x =1.39(1)g cm−3, λ(CuKα)=1.54178 A,μ(CuKα)=21.4 cm−1,F(000)=388 e,T=292K,R=0.066 for 1205 unique reflections. The piperidine ringsA, B, C, andD have chair, chair, boat, and half-chair conformations, respectively. The quinolizidine system (ringsA/B) has atrans configuration. The cations are interconnected by a hydrogen bond O(N1)⋯O(C15) of 2.552(10) A into chains along [010]. Atoms C(12) and C(13) from ringD of the cation are disordered. Very high thermal parameters of the oxygen atoms of the perchlorate anion may indicate its orientational disorder.
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