Abstract
The first crown thioether complexes of SbIII and BiIII, as representative p-block elements, have been isolated, viz SbCl3·9S31, BiCl3·9S3·0.5 MeCN, SbCl3·15S5, 2SbCl3·18S6 2 and BiCl3·18S6; X-ray crystal structure determinations of 1 and 2 establish full participation of ligand S-donor sites in metal ⋯ sulphur bonding in each case.
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