Abstract

Compression creep results in an inert atmosphere are presented for fine‐grained Al2O3–TiN composites deformed under a stress range of 10–50 MPa stress and a temperature range of 1250°–1400°C. The effects of TiN content (10–70 vol%) and the preparation route (i.e., reactive versus nonreactive hot pressing) are considered. Al2O3 and TiN both are efficient grain‐growth inhibitors, relative to each other; thus, deformation develops in stable equiaxed microstructures. Except for low TiN contents (10 and 20 vol%), the processing route does not markedly influence the observed strain rates, at least up to a strain of −0.16. In all cases, deformation occurs mainly via interfacial/grain‐boundary sliding, and its rate is enhanced in approximate proportion to the amount of Al2O3/TiN interfacial area. The deformation rate seems to be limited by either some interface reaction or a complex boundary diffusional mechanism that occurs at the Al2O3 grain boundaries.

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