Abstract
The Front Cover shows the data corresponding to NaTiOPO4 Na-ion anode material obtained in a powder X-ray diffraction operando experiment when cycled between 2.4 and 1V vs Na+/Na (2θ λ Cu = 32° - 34 °, reversible intercalation of 0.58 Na+). Operando experiments have provided key insights regarding the internal processes occurring in a battery during operation and this knowledge has been critical for the design of optimized electrode materials and long-lasting cells. In our work we discuss several experimental considerations that we believe are relevant for operando data acquisition and analysis through different examples collected using our home-made in situ cell using both lab-scale and synchrotron data. More information can be found in the Full Paper by Damien Saurel et al.
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