Abstract
4-Methyltetrahydropyran is a new recyclable ether solvent that can be applied to bench-scale oxidative reactions. During oxidation, however, trace degradation of solvent occurs. Slight amounts of solvent-derived oxidative products were characterized by 1H NMR analyses. The picture shows that the solvent used in the epoxidation reaction contains some degradation products that could be detected in microanalysis. More information can be found in the Full Paper by Shoji Kobayashi and Tomoki Tamura.
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