Abstract
C−H borylation using mechanochemistry has been developed for the first time. Careful choice of the reaction milling jar, ball, and additive enabled the development of a solvent-free iridium-catalyzed C−H borylation reaction that proceeds efficiently in air. Considering the broad significance of C−H borylation processes and the industrial demand for sustainable synthetic methods, the present study constitutes an important milestone toward the development of industrially attractive C−H bond functionalization processes. More information can be found in the Communication by K. Kubota, H. Ito, et al. on page 4654.
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