Abstract
AbstractAn unusual scission–rearrangement process, which couples radical and ionic reactions, was observed with galactofuranose derivatives. This one‐pot procedure afforded, in good yields, highly functionalized 1,4‐dioxanes, which could be considered as six‐membered‐ring sugar analogues. The synthesis of C‐glycoside analogues is also possible with this methodology.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2009)
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