Abstract
Growing blackberries: The association of counterions around {Mo72V30} polyoxometalate macroanions increases with increasing macroion concentration and decreasing solvent polarity. The counterion distribution extends about 2–9 Å from the macroion surface with the highest probability at 2–3 Å from the macroion surface. A close connection between counterion association and the self-assembly of {Mo72V30} into “blackberry” structures is observed.
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