Correlation between Powder Flow Properties Measured by Shear Testing and Hausner Ratio

Abstract

Shear testing provides rigorous estimates of flow properties relevant to the characterization, handling, and processing of powders, and is a necessary test procedure in the formal design of powder storage facilities. However, despite the automation of modern test equipment, it can be time consuming and expensive. In contrast, measurement of bulk density is straightforward and less laborious, and tapping devices are cheaper. Here we explore the relationship between Hausner ratio and cohesion and also examine correlation between Hausner ratio, σc/σy, and σpre for a suite of 13 milled and 2 spray-dried lactose powders, 3 sand samples and 3 samples of refractory dust; Hausner ratio is the ratio of tapped bulk density to loose bulk density, σc is major consolidation stress, σy is unconfined yield stress and σpre is preconsolidation stress. Cohesion and flow function were measured with an annular shear cell at values of σpre up to 5kPa. Loose poured bulk density was measured following a modified New Zealand standard and tapped density measurement was based on a method for dry dairy products and the European Pharmacopoeia; Hausner ratio at 1250 taps was used. Our results show that cohesion at σpre of 0.31kPa, 0.61kPa, 1.20kPa, 2.41kPa, and 4.85kPa correlates linearly with Hausner ratio; the slope and intercept of the correlation are functions of σpre. A plot of σc/σy against Hausner ratio shows an exponential decay trend and regression yields two fitting parameters that correlate well with σpre. These correlations are potentially useful for assessing flow characteristics when shear testing cannot be performed.