Abstract

AbstractA method for site‐selective intermolecular C(sp3)−H thiocyanation of aliphatic sulfonamides is developed using cheap trimethylsilyl isothiocyanate (TMSNCS) as the thiocyanation reagent, catalyzed by simple Cu(I)/phenanthroline complex. The mild, and modular protocol allows remote C(sp3)−H thiocyanation in promising yields with a broad substrate scope.magnified image

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