Abstract
The crystal and molecular structures of a series of structurally related 1,2,3‐triazole‐4,5‐dicarboxylate (LHtzdc = 1,2,3‐triazole‐4,5‐dicarboxylate) ligands for second metal ions were established via single‐crystal X‐ray structural analysis. [Cu (en)]2+ (en = ethylenediamine) was selected as a second metal ion, the two spare sites of the O atom from LHtzdc are coordinated to a single [Cu (en)]2+, and the [Cu (en)]2+ metal centres act as two outer pockets, which is an effective and innovative method of controlling the assembly of heterometallic cages.
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