Abstract

Solid amorphous mixed zirconium-titanium phosphates, with general formula ZrxTi/1−x//HPO4/2.n H2O/ where x=0.1−1, and n=3–5/, are mixed with an excess of solid oxalic acid dihydrate and digested in molten oxalic acid. Then oxalic acid is removed by extraction and the residue washed with dilute /O.OlM/ HCl solution and bidistilled water. As a result of this method, crystalline mixed zirconium-titanium phosphate is formed.

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