Abstract
A convenient and efficient synthesis of 1,6-anhydro-2,4-dideoxy-β-D-threo-hexopyranose (2,4-dideoxy-levoglucosan) from levoglucosan has been developed. The method uses cheap reagents and requires only crystallization and distillation for preparation of pure product on a multigram scale. [Supplementary materials are available for this article. Go to the publisher's online edition of Synthetic Communications® for the following free supplemental resource: Full experimental and spectral details.]
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