Abstract
The hallmark of materials science is the ability to tailor the structures of a givenmaterial to provide a desired response. In this work, the structures involvingcrystallinity and crystallographic orientation of Cu nanowires electrochemicallyfabricated in ion-track templates have been investigated as a function of fabricationcondition. Both single crystalline and polycrystalline nanowires were obtained byadjusting applied voltages and temperatures of electrochemical deposition. Theanti-Hall–Petch effect was experimentally evidenced in the polycrystalline nanowires.The dominant crystallographic orientations of wires along [111], [100], or [110]directions were obtained by selecting electrochemical deposition conditions, i.e.,H2SO4 concentration in electrolyte, applied voltage, and electrodeposition temperature.
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