Abstract
A strategy for the construction of unsymmetrically protected isolated syn 1,2-diols bearing various unsaturated appendages is described. Reaction conditions are described for selective monoaddition to C 2 symmetric 1,2,3,4-diepoxybutane which permits both differential protection of the intermediate epoxy alcohols and a second chain elongation This sequence provides access to unsymmetrical mono-protected diols bearing unsaturated appendages not readily accessible by asymmetric dihydroxylation.
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