Abstract
AbstractThe preparation of alkyl‐ or aryl‐chlorosilanes, extensively studied during the last forty years, is carried out mostly by allowing SiCl4 to act cither on Grignard reagents1 or on alkyl‐zinc or mercury‐compounds.2 The. Fittig‐Wurtz method for the preparation of tetra‐substituted deri‐vates was first utilized by Polis3 and later by Kipping and Lloyd.4 Schumb, Akermann and Saffer found it practical to preparathe sodium organic derivative separately and then to treat‐it with the silicon halide. The action of Grignard reagents on ethyl silicate has been studied particularly by Russian chemists5.
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