Continual preparation of chemical vapor standard mixtures: Autonomous generator based on modified dynamic methods

Abstract

Many applications in laboratory, industrial and R&D practice involve utilization of standard chemical vapor mixtures, therefore their availability, ease of preparation and reliability play a crucial role. This work is presenting a new instrumentation based on the innovated dynamic preparation method using the injection of liquid sample, fast evaporation, and uniform mixing with carrier gas. The combination of precise syringe drives, quantitative evaporation and controlled flow of carrier gas provides very high level of accuracy and stability of the generation process. The system is robust with minimal requirements for calibration, and it is suitable for producing single or multi component mixtures.