Abstract

A new energy dispersive diffractometer has been developed. It consists of a solid tungsten carbide conical collimator and a large area annular detector. Diffracted intensities are increased by at least one order of magnitude. Developed for high-pressure studies and their microsamples, the instrument will improve the accuracy of intensity measurements by reducing crystallite statistics effects and the collection of a complete cone of diffraction will greatly facilitate high-pressure single-crystal studies. The results of the first test of the instrument are reported.

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