Abstract
Detailed conformational analysis of 1-phenyl-1H-4,5-dihydro-2,4-benzodiazepines using X-ray structures, nuclear Overhauser experiments, variable-temperature 1 H NMR, and MacroModel (MULTIC) reveals a rapid equilibrium between axial and equatorial comformations for the free base of 2. The DCl salt of 2 and 1-methyl-1-phenyl analog 3, however, prefer the axial conformation
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