Abstract
An improved method for synthesizing the compounds K2MoxW1−xO4has been applied. The phase diagram, both on heating and cooling, is presented. The observed nearly linear character of the concentration dependence of the modulation parameterpat 693 K (both after heating and cooling) indicates the existence of a continuous series of incommensurate structures in the concentration interval 0 ≤x≤ 1. Either atx= 0 exactly or close to this value a lock-in phase transition takes place, making the structure commensurately modulated.
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