Abstract
The new esculetin (H 2esc; 6,7-dihydroxy coumarin) complexes cis-[MO 2(esc) 2] 2−, [M 2O 5(esc) 2] 2− (M = Mo, W), trans-[UO 2(esc)·MeOH], trans-[OsO 2(esc) 2] 2−, [M(esc) 3] 2− (M = Os, Re, Ir), [M(esc) 3] 3− (M = Fe, Rh), [Ru(bipy)(esc) 2], [ML(esc)] [M = Pd, Pt; L = (PPh 3) 2, bipy] and [ReOI(PPh 3) 2(esc)] have been prepared. Their Raman, IR, 1H and 13C NMR and mass spectra have been measured, and cyclic voltammograms of some of them recorded.
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